diff --git a/assays/ProteinPull-down/protocols/BiotinylationOfLaminarin.md b/assays/ProteinPull-down/protocols/BiotinylationOfLaminarin.md new file mode 100644 index 0000000000000000000000000000000000000000..4a0640ca4b2acb3535694c4bbb7416cad8b274ef --- /dev/null +++ b/assays/ProteinPull-down/protocols/BiotinylationOfLaminarin.md @@ -0,0 +1,2 @@ +## Biotinylation of laminarin +Laminarin (final concentration ∼ 60 mM) was incubated with biotin-hydrazide (120 mM) and sodium cyanoborohydride (1 M) for 2 h at 65 °C. The product was purified on a PD MidiTrap G-10 column (GE Healthcare) according to the manufacturer’s description. Success of biotinylation was validated via mass spectrometry. The immunogenic capacity of biotinylated laminarin was confirmed via ROS burst assays. \ No newline at end of file